MICROSTRUCTURALLY INFORMED HIGH-VELOCITY IMPACT EXPERIMENTATION ON ADDITIVELY-MANUFACTURED METALLIC MATERIALS

This work presents a flexible experimental setup to study dynamic fragmentation of additively-manufactured metallic materials using two different configurations: (i) rapid axial penetration of thin-walled tubes, and (ii) rapid radial expansion of rings. In the first approach, the experiment consists of a light-gas gun that fires a conical nosed cylindrical projectile that impacts axially on a thin-walled cylindrical tube fabricated by 3D printing. The diameter of the cylindrical part of the projectile is approximately twice greater than the inner diameter of the cylindrical target, which is expanded as the projectile moves forward, eventually breaking into fragments. In the second approach, using a similar technique, a ring is inserted over a high-ductility tube, which expands after penetration by the conical projectile, pushing the metallic ring radially outwards, ultimately breaking into multiple fragments. The experiments have been performed for impact velocities ranging from 180 m/s to 390 m/s. A salient feature of this work is that we have characterized by X-ray tomography the porous microstructure of selected specimens before and after testing. Moreover, two high-speed cameras have been used to film the experiments and thus to obtain time-resolved information on the mechanics of formation and propagation of fractures.
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VERY HIGH-CYCLE FATIGUE BEHAVIOR OF ADDITIVELY MANUFACTURED TI-6AL-4V USING ULTRASONIC FATIGUE MACHINE AND SELF-HEATING TESTING.

Accelerated characterization of high-cycle fatigue properties is necessary in order to enable the optimization of parameters of additive manufacturing processes such as LPBF (Laser Powder Bed Fusion). Therefore, two accelerated characterization methods are applied and compared on Ti-6Al-4V samples produced using the LPBF process. The first method uses an ultrasonic fatigue machine and the second one determines the fatigue limit using self-heating testing. To study the interactions between the material and the accelerated testing methods, fatigue tests are carried out on different grades of Ti-6Al-4V-LPBF differing by their microstructure or their porosity. Three grades have the same microstructure but different porosity levels and three grades have different microstructures with the same porosity. Both properties showed a strong impact on VHCF strength and affected the mechanisms at fatigue crack initiation.
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CRACK GROWTH-BASED FATIGUE-LIFE PREDICTION OF ADDITIVELY MANUFACTURED MATERIALS

In this study, a plasticity-induced crack closure model, FASTRAN, was used to predict the fatigue life of Inconel 718, 17-4 precipitation hardening (PH) stainless steel (SS), and Ti-6Al-4V alloys fabricated via additive manufacturing (AM) systems. Results indicated that in the presence of large defects (e.g., lack-of-fusion defects), the total fatigue life of AM specimens is dominated by crack growth. Results indicated that variations in the fatigue lives of specimens in machined and as-build surface conditions can be predicted based on the characteristics of AM process-induced defects and surface profile. Effect of build orientation on fatigue life was also captured based on the size of defects projected on a plane perpendicular to the loading direction. In addition, maximum valley depth of the surface profile can be used as an appropriate parameter for the fatigue-life prediction of AM specimens in their as‐built surface condition.
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ANALYSIS OF POROSITY EFFECTS ON SPALL FAILURE OF ADDITIVELY MANUFACTURED 316L SS

Additive manufacturing (AM) allows for tuning of mechanical properties for unique functionalities, and stainless steel is a prime candidate for use in many applications due to its high strength, ductility, and corrosion resistance. AM fabricated 316L stainless steel samples with intentionally random pore placement are compared to samples with known pore placement to study the interaction of the shock wave with individual and grouped pores. Velocity profiles were obtained using photon doppler velocimetry (PDV) probes placed strategically along the location of the known pores to understand the limits of local influence for the known pores. Post-mortem characterization of soft-recovered samples using electron backscatter diffraction (EBSD) and transmission electron microscopy (TEM) was performed to investigate the strain accommodation around pores. It was observed that shock wave fronts are highly dispersed and slow as they propagate through the pore due to strain accommodation around individual pores. As a result, there is shifting of the spall plane away from the impact face. This slow wave front propagation also results in slow rise time and lack of velocity plateau in the collected velocity profiles when areas with pores were probed.
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INFLUENCE OF THE CONTOUR PARAMETER IN MICROSTRUCTURE DUALITY AND FRACTURE INITIATION IN NON-COMBUSTIBLE MAGNESIUM ALLOYS FABRICATED BY LASER POWDER BED FUSION

Non-combustible Mg alloy components fabricated by laser powder bed fusion in as-built conditions have an average ultimate tensile strength (UTS) of 320 MPa, a significantly larger value than its casting counterparts, which present an average UTS of 200 MPa. In addition, it was determined that stable crack extension always starts at the outer surface due to the coarsened microstructure regions present in the area. Therefore, this paper will use fracture mechanics to predict the UTS value by determining the size of the coarsened microstructure region and considering it as a surface crack with the √area parameter. Then, by using a fixed fracture toughness value, the UTS will be predicted. Furthermore, a processing parameter known as contour, which is used for remelting the outer surface of the specimen, can also smoothen the microstructure and potentially increase the UTS value. Results showed that the √area of the surface crack responsible for fracture was 730 μm for the no-contour specimen and 630 μm for a contour specimen. Subsequently, using Murakami’s theory, the predicted UTS is 320 MPa and 345 MPa respectively. Finally, tensile testing was performed to confirm the prediction, showing similar results with an average deviation of 2.9%.
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FAILURE CHARACTERIZATION IN 17-4PH STAINLESS STEEL ACROSS MULTIPLE MANUFACTURING METHODS

Accurate models of additively manufactured (AM) materials require extensive mechanical testing for proper calibration and verification/validation. The process-structure-property relationships in 17-4PH stainless steel from multiple manufacturing modes were examined via mechanical testing across several strain rates and post-mortem characterizations of the fracture surfaces and microstructure. Under all manufacturing modes and testing conditions, optical and scanning electron microscopy showed ductile failure characteristics. Higher porosity concentration (determined by density measurement) resulted in lower ultimate strength in cast samples; the pores often acted as crack initiation points. Strain-rate dependence and failure modes were also affected by process-dependent anisotropy in the microstructure, which was quantified through electron backscatter diffraction (EBSD) imaging. This data will be used to inform models of failure in the 17-4PH for multiple manufacturing forms.
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EVALUATION OF STRENGTH CHARACTERISTICS FOR NON-COMBUSTIBLE MAGNESIUM ALLOY PRODUCTS FABRICATED BY LASER POWDER BED FUSION UNDER AS-BUILT CONDITION

It is difficult to evaluate fracture toughness according to ASTM standards for non-combustible magnesium alloy fabricated by Laser Powder Bed Fusion (LPBF) in as-built conditions. The reason is its microstructure duality between inner and outer surfaces. The microstructure duality can be eliminated by heat treatment. However, heat treatment reduces the strength of the material by around 11%. Therefore, heat treatment was not performed. In addition, the greatest advantage of LPBF is maximized when it can be used immediately without post-processing. Therefore in this study, the as-built condition was targeted. In the case of non-combustible Mg products, the mechanical properties of the inner and outer microstructures have a non-negligible difference. The difference is expected to affect the fracture behavior, so it is important to consider the difference in microstructure in strength evaluation. Therefore, this paper explains why ASTM standards are difficult to apply to non-combustible magnesium products fabricated by LPBF in as-built conditions with their microstructure differences. Furthermore, the alternative methods for measuring the fracture toughness of metals fabricated by the LPBF in as-built conditions with these characteristics are introduced and discussed.
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MODELING OF MIXED-MODE CRACK GROWTH BEHAVIOR IN LB-PBF TI-6AL-4V USING A CRITICAL PLANE FRAMEWORK

Many service loading conditions are multiaxial, and small cracks have been shown in many situations to grow in mode II or mixed-mode due to the orientation of defects and microstructural effects, particularly in additively manufactured metals. This paper uses fracture mechanics with a critical plane framework to predict crack growth rates using only mode I constants from the literature.
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REDUCING LOW CYCLE FATIGUE LIFE SCATTER OF ADDITIVE MANUFACTURED ALSI10MG USING LASER SHOCK PEENING

Additive manufactured (AM) alloys are still prone to critical manufacturing flaws, such as gaseous bubble entrapment. These defects can lead to early crack initiation reducing fatigue life and increasing scatter, especially when near surface. This research investigated the effect of femtosecond laser shock peening (FLSP) on the fatigue life of AM AlSi10Mg. Due to the low penetration of the FLSP, fatigue life remained consistent between treated and untreated specimens. Of equal importance though, the scatter was found to be reduced in the FLSP treated samples. From the high resolution DIC results, the average strain per grain in the untreated specimens showed a higher increase of strain from initial loading to final fracture as compared to the FLSP samples. Implementing the use of FLSP onto AM materials could lead to more consistent fatigue life despite the presence of porosity, leading to a path of easier certification and improved confidence in their behavior.
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SIGNIFICANCE OF INTRA-BUILD DESIGN VARIABLES ON THE FRACTURE TOUGHNESS PROPERTIES OF ELECTRON BEAM MELTED TI6AL4V

Structurally reliable materials are essential for adopting additive manufacturing (AM) metals in safety-critical applications. Limited data on the damage-tolerance properties of metal AM materials exists, hindering the acceptance of AM metals in fracture-critical applications. A design of experiments (DOE) is used in this study to investigate the role of build space and part design parameters on the fracture toughness properties of Electron Beam Melted (EBM) Ti6Al4V. ASTM E399 tests were performed on over 100 compact tension (CT) samples in the as-built and machined conditions to obtain fracture toughness properties and evaluate the influence of part size and location within 80% of the build space. Results were comparable to wrought annealed titanium, with less than 10% variation in overall fracture toughness. Specimen location within the build envelope contributed to the observed variation, with an increase in properties with build height and specimens located in the center of the build envelope. The location-dependent properties result from changes in microstructure and porosity throughout the build space. While the experimental EBM Ti6Al4V fracture toughness properties are promising for future applications, it is crucial to consider the variation in properties due to build space location and design parameters when designing for consistency.
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